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    Columnar to Equiaxed Transition in Spot Melt Electron Beam Powder Bed Fusion Scan Strategy and Utilization of Microstructure Informatics

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    Author
    Madigan, Michael Edward
    Issue Date
    2025
    Keywords
    Columnar to Equiaxed Transition
    Electron Backscatter Diffraction
    Electron Beam Powder Bed Fusion
    Microstructure
    Microstructure Informatics
    Spot Melt
    Advisor
    Tin, Sammy
    
    Metadata
    Show full item record
    Publisher
    The University of Arizona.
    Rights
    Copyright © is held by the author. Digital access to this material is made possible by the University Libraries, University of Arizona. Further transmission, reproduction, presentation (such as public display or performance) of protected items is prohibited except with permission of the author.
    Abstract
    Electron beam powder bed fusion (EB-PBF) has significant potential for achieving controlled microstructural development in additively manufactured components while addressing anisotropic mechanical property limitations inherent to conventional powder bed fusion processes. This work evaluated the columnar-to-equiaxed transition behavior and microstructural refinement characteristics of spot melt scanning strategies in EB-PBF processing. IN718 specimens were processed using four distinct scanning patterns and subjected to comprehensive microstructure informatics analysis to examine relationships between processing parameters, thermal management, and resulting grain morphology characteristics. Specimens underwent systematic beam current and dwell time variations to investigate the influence of energy density on microstructural evolution mechanisms. In addition, traditional raster scanning was examined to provide context for comparison with the experimental spot melting approaches. Microstructural characterization was performed using electron backscatter diffraction (EBSD) combined with quantitative informatics methodologies, in which comprehensive statistical analysis of grain dimensions and aspect ratios was conducted to establish processing-structure relationships. Aspect ratio measurements for the spot melting specimens were found to vary by factors of two to four compared with traditional raster scanning results, demonstrating the effectiveness of temporal separation strategies for columnar-to-equiaxed transition control. Scanning pattern configuration did not indicate a significant impact on densification behavior when adequate energy density was maintained. Moreover, equiaxed microstructural development appeared predominantly in specimens with optimized temporal separation between adjacent melt events as confirmed through three-dimensional EBSD reconstruction analysis. The work presented provides systematic assessment of the relationship between spot melting processing conditions, resulting microstructural characteristics, and thermal management strategies, while offering insight into development pathways for improved mechanical isotropy in this technologically important manufacturing process.
    Type
    text
    Electronic Thesis
    Degree Name
    M.S.
    Degree Level
    masters
    Degree Program
    Graduate College
    Materials Science & Engineering
    Degree Grantor
    University of Arizona
    Collections
    Master's Theses

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